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Journal Articles

Study on magnetic property change on neutron irradiated austenitic stainless steel

Nemoto, Yoshiyuki; Oishi, Makoto; Ito, Masayasu; Kaji, Yoshiyuki

Nihon Hozen Gakkai Dai-12-Kai Gakujutsu Koenkai Yoshishu, p.105 - 112, 2015/07

Authors previously reported that Eddy current method and AC magnetization method have potential to be applied for development of diagnostic technics to detect the sign of material degradation before cracking on the austenitic stainless steels used as structural material in nuclear power plants. In typical austenitic stainless steels such as type304, magnetic ferrite phase would exist in the alloy before irradiation, and it is concerned to disturb the magnetic measurement on irradiated material. Magnetic measurements were conducted in this work on type304 austenitic stainless steel specimens irradiated up to different doses. In addition, microstructure observation was conducted on the area including grain boundary to discuss the correlation of magnetization on irradiated austenitic stainless alloy and grain boundary cracking. Obtained magnetic data on irradiated type304 stainless steel were seen clearly different from that on un-irradiated specimen, and showed positive correlation with radiation dose, therefore it was thought that magnetic measurement technics can be applied for the material which contains certain quantity of ferrite phase before irradiation. In the microstructural observation, magnetic phase (FeNi$$_{3}$$) formation along the grain boundary was revealed.

Journal Articles

Development of analytical method and study about microstructure of oxide films on stainless steel

Nemoto, Yoshiyuki; Miwa, Yukio; Kikuchi, Masahiko; Kaji, Yoshiyuki; Tsukada, Takashi; Tsuji, Hirokazu

Journal of Nuclear Science and Technology, 39(9), p.996 - 1001, 2002/09

 Times Cited Count:6 Percentile:39.48(Nuclear Science & Technology)

Surface morphology of oxidized stainless steel was evaluated using atomic force microscope (AFM) and scanning electron microscope (FE-SEM). Cross-sectional morphology of oxide layer on the specimens was evaluated using FE-SEM after fabrication. Focused ion beam (FIB) technique was applied to fabricate thin film samples of oxide films, which were used for microstructure observation by transmission electron microscope (FE-TEM), and microscopic chemical analysis by energy dispersed X-ray spectrometer (EDS). These preparations and observations were successful, and microstructure and chemical composition of oxide films were evaluated on nanometer scale. Effects of silicon (Si) doping and dissolved oxygen (DO) content in water for oxide layer formation are discussed.

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